Předmět Separační procesy (N111016)

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Materiál	Typ	Datum	Počet stažení

Sylabus

Syllabus 1. Introduction and the course justification Specific position of small-scale technologies in chemical industry, features of pharmaceutical processes, scale-up in engineering of pharmaceutical processes, design and optimization of batch processes, more complex cases of process development2. Material and Enthalpy Balances Rules for formulation of balances, derivation of equations, a typical apparatus - a column with the counter-current flow of phases, solution of equations 3. Liquid Extraction (Solvent Extraction) Solvent selection, types of extractors, process design, mass balance, solutions of non-linear equations, a case study4. Solid -- Liquid Extraction (Leaching, Percolation, Infusion) Definition (mechanism, process methods), examples of applications, types of extractors, process design, mass balance, numerical solution of non-linear equations, process control, an example of calculation5. Supercritical Extraction Definition, thermodynamic basis, types of extractors, process design, process control, industrial applications6. Liquid Chromatography Introduction and definitions, classification, techniques (methods), equipment, stationary and mobile phases7. Adsorption Definitions and basic quantities, Gibbs adsorption isotherm, models of adsorption isotherms, multicomponent adsorption isotherms, estimation of isotherm parameters8. Preparative Liquid Chromatography Models of chromatographic columns, process design, equilibrium data acquisition9. Adsorption Processes Microporous adsorbents, basic characteristics of the processes, cyclic batch systems (CBS), desorption (regeneration) methods for CBS, continuous countercurrent systems (CCS), comparison of chromatographic processes and CCS10. Freeze Drying (Lyophilization) Introduction, benefits of freeze drying, freezing, freeze drying, rates of freeze drying, process equipment11. Membranes and Mass Transfer Introduction, fundamentals, principles of membrane processes, mass transfer in membranes, types of membranes12. Membrane Separation Processes Types of membrane processes, preparation and membrane module construction, concentration polarisation and membrane fouling 13. Crystallisation Basic definitions, phase equilibrium, basic balances, formation of nuclei, kinetics of crystal growth, hydrodynamic properties of suspensions, control of crystal shape, product properties, methods of crystallisation, sublimation and desublimation14. Crystallisers classification of crystallisers, design of crystallisers

Literatura

Z: J. Hanika: Speciální separační procesy, skripta VŠCHT, Praha (1998), 80-7080-242-1.Z: J. D. Seader, E. J. Henley: Separation Process Principles, 2nd edition, John Wiley & Sons, New York (2006), 0470481838.D: R. B. Bird, W. E. Stewart, E. N. Lightfoot: Transport Phenomena, 2nd edition, John Wiley & Sons, New York (2007), 0470115394.D: R. C. Reid, J. M. Prausnitz, B. E. Poling: The Properties of Gases & Liquids, 4th edition, McGraw-Hill, Boston (1987), 0470115394.D: D. M. Ruthven: Principles of Adsorption and Adsorption Processes, John Wiley & Sons, New York (1984), 0471866067.D: R. Taylor, R. Krishna: Multicomponent Mass Transfer, John Wiley & Sons, New York (1993), 0471574171.

Garant

Čapek Pavel doc. Ing. CSc.